ICMCTF2008 Session E4/G4: Tribological Studies of Coatings for Green Manufacturing and Dry Machining

Wednesday, April 30, 2008 1:30 PM in Room California

Wednesday Afternoon

Time Period WeA Sessions | Abstract Timeline | Topic E Sessions | Time Periods | Topics | ICMCTF2008 Schedule

Start Invited? Item
1:30 PM E4/G4-1 Evaluation of Nanomechanical Test Approaches Towards PVD Coating Optimisation for High Speed Machining of Steel
B.D. Beake (Micro Materials Ltd, United Kingdom); G. Fox-Rabinovich (McMaster Unviersity, Canada)
A plasticity index (PI), the plastic work done/total work done during indentation is related to the ratio of hardness to modulus. Its use to predict the life of coated WC-Co tools with hard PVD coatings in various mechanical contact conditions such as high speed interrupted cutting (turning and milling) has been investigated. A correlation between this index and the severity of the cutting conditions is observed suggesting the PI determined from nanoindentation can be used as a first approximation in determining whether or not a PVD coating could have the desirable mix of mechanical properties for a given cutting application. However, in tool operation increased plasticity (higher PI) is accompanied by several other factors, which may or may not be beneficial and the influence of these on tool life is discussed. Some of the limitations of the plasticity index as a sole predictor of coating performance can be addressed by performing additional novel nanomechanical tests, such as micro-and nanowear, elevated temperature nanoindentation and nano-impact. These are introduced with a discussion of their regimes of usefulness for simulation and prediction of coating performance. Nano-impact correctly ranks coatings in terms of tool life in end milling and reproduces the shapes of the tool wear vs. cutting time traces. Elevated temperature nanoindentation on tool coatings reveals the PI increases with temperature, particularly when a loss of coating stability occurs in addition to thermally activated dislocations. In elevated temperature nano-impact tests probability and extent of fracture decrease markedly as temperature increases, consistent with the higher PI. The results can be used to predict which coatings have longer life in interrupted cutting conditions.
1:50 PM E4/G4-2 Cathodic Arc Ion Plated Cr2O3 Coating for Dry Cutting Tool Applications
K. Sato, Y. Tanaka (Mitsubishi Materials Corporation, Japan)
Cr-O coatings were deposited on WC-Co substrates by using the cathodic arc ion plating method. The structures and the compositions were characterized by X-ray diffraction (XRD), electron probe microanalysis (EPMA) and transmission electron microscopy (TEM) and the mechanical properties were evaluated by Vickers indentation tests and ball-on-disk wear tests. The structure and hardness of Cr-O coatings, measured by XRD and Vickers indentation tests, were found to vary significantly with the oxygen flow rate during the deposition. Cr2O3 coating with the corundum structure had a dense microstructure with the hardness of up to 30GPa and much lower friction coefficient for steel than nitride coatings at elevated temperatures in air. Cutting performance of Cr2O3 coated carbide endmills were evaluated and offered significantly better performance in the high speed machining of steels even with dry conditions. Wear mechanism and cutting characteristics were discussed with the microstructure and properties of the Cr2O3 coatings.
2:10 PM E4/G4-3 Surface Properties and Tool Performance of WC-Co Micro-Drill by Nitrogen Ion Implantation
S.H. Shin, M.C. Kang, Y.K. Jeong, D.H. Kim, K.K. Kim, J.S. Kim (Pusan National University, Korea)
High-speed micro-drilling is an economic method to machine micro-holes with goods precision, and is suitable for machining many kinds of work-piece materials. Cemented carbide (WC-Co) are used in a variety of important industrial components and parts, such as inserts tip, drill, end-mill, mechanical face seals, submersible pumps, and so on. Surface modification of industrial materials and tools is of grate interest in industry, and ion implantation is one of the more effective techniques. In this study, nitrogen ions were implanted into WC-Co substrates which would be used for lifetime improvement of micro-drill and nitrogen ion distribution profile were analyzed by Auger Electron Spectroscopy (AES). To analyze the modified surface, properties such as micro hardness, friction coefficient, wear resistance and surface roughness were measured. Micro hardness of ion implantation specimens was higher than that of un-implanted specimens. Friction coefficient was reduced, and wear resistance was improved. The tool performance of micro-drill was evaluated by drilling of Al6061-T6 using un-implanted and implanted WC-Co cutting tools. Consequently, micro-drill made from nitrogen ion implantation showed excellent performance under high-speed cutting condition. The reliable evaluation system for tool wear measurement of micro-drill was newly designed.
2:30 PM E4/G4-4 Successful Utilisation of Tribological Coatings for Green Manufacturing and Dry Machining
M. Larsson (Primateria, Sweden)

The gradually stricter environmental regulations and their enforcement are eliminating much of the flexibility in the use of cutting fluids and lubricants in the metal machining industry. Therefore manufacturers of cutting fluids and lubricants are developing new formulations, for example formulations without the elements Pb, S, or Cl which improves machinability but are detrimental from a health and environmental point of view. It is, however, a long way to go before these new lubricants can be considered completely harmless and acceptable. Furthermore, the cost associated with the use of cutting fluids is estimated to be several billion dollars per year. Consequently, reducing the use of cutting fluids or metal forming lubricants, i.e moving towards so called green manufacturing (environmentally friendly manufacturing), can be a considerable economic motivation for the metal machining industry.

One approach towards dry machining is to improve the properties of the tool material by making them more wear resistant, i.e. more refractory and/or to make tools that generate less friction heat during machining. There has been a continuous development of tool materials over the past century starting with high-speed steels, cast cobalt alloys, cemented tungsten carbide, ceramics, coated carbides and coated HSS, cubic boron nitride and diamond, i.e. towards more and more heat and wear resistant materials. It is very often forgotten though, that these more advanced tool materials also are becoming more and more brittle as compared to traditional tool steel materials. It is also too often forgotten that coated tools can not be subjected to an excessive wear during break in of the tool, if the coating should be able to protect the less wear resistance substrate material in a reliable and predictable way. Hence, it is important to optimise not only the inherent properties of new tool materials but also the brittle substrate and coating composite. This should be done with the goal to obtain excellent resistance against thermal and mechanical wear without jeopardizing the reliability of the tool. A reliable tool is a prerequisite for high productivity and successful utilisation of advanced tool materials, which in turn is a prerequisite for green manufacturing. The question is how to do this? Until today, too little attention has been given to this subject, i.e. optimisation of a given tool, including the tool material (substrate) and the coating, with respect to its ability to carry load (thermal or mechanical) and how such an optimisation affects the reliability and useful life of the tool. The presentation will focus on how to optimise the performance of coated tools with respect to their ability to carry load and increase tool life in a predictable way to avoid excessive wear, premature brittle fracture or fatigue wear of coated (as well as uncoated) tool materials.

3:10 PM E4/G4-8 Correlation of the Impact Resistance of CrAlN PVD Coatings With the Cutting Performance in Milling Aerospace Alloys
K.-D. Bouzakis, N. Michailidis, S. Gerardis, G. Katirtzoglou, E. Lili, M. Batsiolas (Aristoteles University of Thessaloniki, Greece); M. Brizuela, A. Garcia-Luis (Fundación Inasmet-Tecnalia, San Sebastian, Spain); R. Cremer (CemeCon AG, Germany); H.G. Fuß (CemeCon, Germany)

The present paper proposes a novel methodology based on analytical and experimental test methods for predicting coated tool efficiency in milling Inconel 718 and Ti6Al4V, using coated cemented carbide inserts. The applied coatings were CrAlN coatings, containing or not Zr or Y dopants. The stress-strain curves and the fatigue critical loads at various temperature levels of these coatings were determined by nanoindentations and impact tests respectively, employing various FEM-supported procedures for results evaluation. In this way coatings’ Woehler diagrams were established for specific film operational temperatures.

The milling investigations were conducted at various cutting speeds and feedrates. An insight of the developed stress and temperature fields in the cutting wedge region, during the milling process at various cutting conditions, was obtained by force measurements and calculations, based on FEM-simulations of the material removal.

These results, along with FEM-based calculations of the cutting wedge thermal and mechanical loads during the material removal process, facilitated the explanation of the coated inserts’ cutting performance at various conditions. The obtained results revealed a sufficient correlation of the coatings’ impact resistance at various temperatures with the cutting performance at corresponding cutting speeds.

3:30 PM E4/G4-9 Abrasiveness Properties Assessment of Coated Abrasives for Precision Belt Grinding
S. Mezghanim, M. El Mansori (Laboratoire de Mécanique et de Procédés de Fabrication (LMPF, EA 4106), France)
This paper addresses a study to achieve a method of assessment of coated abrasives for precision belt grinding based on the identification of the prevailing relationships between the changing features of fixed grains on flexible coated belts and grinding performance. A set of parameters was defined which describe the aluminum oxide resin-bonded belt characteristics including active grits density, cutting edge dullness, chip storage space and mean effective indentation. A parametric study was made of the effects of coated belt characteristics on surface finish performance with different grain sizes and contact pressure values for grinding different workpiece materials. Experimental results are discussed in relation to the prevailing physical mechanisms of the process at the beltwork interface which can be separated into chip formation, ploughing and friction components. These mechanisms are then correlated to selected multiscale parameters which result from the multiscale analysis of the changing topographically features of the machined surface. This is enables also to describe the grit wear mechanisms operating with coated abrasives when grinding a variety of engineering materials. Suggestions are finally made for the choice of optimal grit size of coated belt using a new assessment criterion.
3:50 PM E4/G4-10 Synthesis, Properties and Cutting Performance of the (Al,Cr)2O3 Coatings Produced by Cathodic Arc Evaporation
D. Kurapov, F. Fontaine, J. Ramm, M. Ante, T. Bachmann (OC Oerlikon Balzers AG, Liechtenstein); M. Doebeli (Paul Scherrer Institute and ETH Zurich, Switzerland); O. Massler (OC Oerlikon Balzers AG, Liechtenstein)
Al2O3 coatings have been employed for many years for the protection of cutting tool surfaces because of their outstanding high temperature stability and chemical wear resistance. For cutting applications with operation temperatures in excess of 1000°C the thermodynamically stable α- Al2O3 is often preferred. Nowadays commercially available α- Al2O3 can be produced mostly by chemical vapour deposition (CVD) process at a temperature above 1000°C. Recently (Al,Cr)2O3 coatings with α-type crystallographic structure were produced utilizing pulse enhanced cathodic arc evaporation. The properties of the α-(Al,Cr)2O3 are believed to be similar to α-Al2O3 which makes this type of coatings promising for using for metal cutting applications. Here we report on the further progress in the development of the α-(Al,Cr)2O3 coatings deposited utilizing cathodic arc evaporation. The (Alx,Cr1-x)2O3 coatings with x=0-0.7 were produced in the temperature range of 450-600°C. The coatings were analysed with respect to their stoichiometry by means of Rutherford backscattering spectroscopy (RBS). The evolution of the crystallographic structure as a function of chemical composition and deposition temperature was studied by X-ray diffraction (XRD). The morphology of the coatings was analyzed by scanning electron microscopy (SEM). Mechanical properties of the coatings were measured by nanoindentations. Finally the results of the cutting tests are presented.
Time Period WeA Sessions | Abstract Timeline | Topic E Sessions | Time Periods | Topics | ICMCTF2008 Schedule