ICMCTF2013 Session G4-1+E: Coatings for Machining Advanced Materials and for use in Advanced Manufacturing Methods

Monday, April 29, 2013 10:00 AM in Room California

Monday Morning

Time Period MoM Sessions | Abstract Timeline | Topic G Sessions | Time Periods | Topics | ICMCTF2013 Schedule

Start Invited? Item
10:00 AM G4-1+E-1 Advanced Coatings and Tool Materials for Hobbing - a Major Step Forward in Productivity
Philipp Immich, Uwe (U.) Kretzschmann, Matthias Rommel, Thomas Falk, Ronny Fischer (LMT Fette Werkzeugtechnik GmbH & Co. KG, Germany)

Today without gear wheels almost nothing is turning. Manufacturers produce these components by the million for use in automotive gearboxes or in the gears of large wind turbines. Gear hobs have proven themselves for more than a hundred years now in the manufacture of gear wheels and other tooth-cutting tasks.

The ever increasing demand for higher productivity in manufacturing gears requires advanced hard coatings and new substrate materials. Up to now in this field of gear hobbing different substrate materials are used for single-piece hobs: powder metallurgy high-speed steel (PM-HSS) and cemented carbide. Today PM-HSS has a market share around 70% offering limited cutting speeds for wet and dry conditions. On the other hand cemented carbide offers strong performance related features like high cutting speeds up to 400 m/s. But due to the fact, that hobs have a typical life cycle time of 10-15 recondition cycles– hobs are often demounted – packed and shipped – decoated- regrinded and coated again- could cause small handling or production damages that result in a shorter tool life time and less reliability of the production process.

On the substrate side – there is a new generation of intermetallic phase substrate on the market offering compared to conventional PM-HSS higher hot hardness and as result from these higher cutting speeds. On the coating side the development focus is on introducing new coatings allowing new cutting features. In fact today hobs are coated and e.g. dry gear cutting is only possible with coated tools due to the prevention of chip welding. Today hob coatings that are available on the commercial market mainly based on TiAlN system. Now there is a significant switch in the market towards the system Cr-Al-N offering higher oxidation resistance and higher wear resistance. As a result of these developments it is possible to increase cutting speeds up to 50% compared to conventional coatings

For large modules hobs with inserts are offering an economic way of producing gears. There are gear milling cutters (single tooth method) and ICI hobs available. The selection of the best type of tool depends on the lot size to be manufactured and the corresponding number of teeth. Gear hobbing is the most productive method for cutting large-module gears with a high number of teeth. Gear milling cutters are especially to be preferred for low numbers of teeth or small lot sizes. In the last years the performance of these tools are driven by new cutting material grades like new ultra-fine grain carbide combined with new thick PVD coatings and special micro-surface preparation.

10:40 AM G4-1+E-3 Physicochemical, Mechanical and Tribological Properties of Si3N4-MoS2 Thin Films Deposited by Magnetron Sputtering
Ronaldo Trentin, Aline Bandeira, César Aguzzoli, Israel Baumvol, María Moré Farias, Carlos Figueroa (UCS - Caxias do Sul University, Brazil)

Hard coatings are widely used in surface engineering for wear protection of tools and mechanical components. Nowadays, dry machining technologies are emerging techniques due to both saving costs and environmental issues. Such type of coatings to be applied in tools for dry machining must combine not only high hardness and structure stability but also tribological aspects like ultra-low friction. Si3N4 thin films show outstanding performance, in terms of wear and corrosion resistance, in cutting tools at higher temperatures than 1000 oC. However, the incorporation of MoS2 in Si3N4 thin films could reduce the friction coefficient maintaining high values of hardness in these thin films.

In this work, Si3N4-MoS2 thin films were deposited on Si(100) substrates by dual rf and dc reactive magnetron sputtering from Si and MoS2 targets in a Ar/N2 plasma with different MoS2 amounts. The composite thin films were characterized by glancing angle X-ray diffraction, Rutherford backscattering spectrometry, glow-discharge optical emission spectroscopy, nanohardness at different temperatures (23oC to 400oC) and nano-scratch and friction measurements at room temperature. In the whole layer both Si3N4 and MoS2 compounds are stoichiometric and the deposition rate is 0.12 nm.s-1. Moreover, the structure is amorphous and homogenous. The MoS2 content in the composite thin film goes from 0.2 at. % to 4 at. %. In contrast to previous results where the hardness of the TiN-MoS2 nanocomposite system decreases monotonously following the mixture rule when MoS2 is incorporated, our Si3N4-MoS2 thin films show a maximum hardness of 28.5 ± 1.5 GPa at a MoS2 content of 1.6 at. %. The hardness of these Si3N4-MoS2 thin films decrease slightly as a function of temperature. Finally, the friction coefficient tendency of the Si3N4-MoS2 thin films will be discussed and compared to the TiN-MoS2 nanocomposite system where a minimum friction coefficient is reached at intermediate MoS2 contents.

11:00 AM G4-1+E-4 Effect of Silicon Content on Pvd Nitride Film Mechanical Properties and Cutting Performance of Coated Cemented Carbide Inserts
Konstantinos-Dionysios Bouzakis (Aristoteles University of Thessaloniki, Greece); Emmanouil Bouzakis (Fraunhofer Project Center for Coatings in Manufacturing (PCCM), Greece); Spiros Kombogiannis, Georgios Skordaris, Stylianos Makrimallakis, Michail Batsiolas (Aristoteles University of Thessaloniki, Greece); Rachid M’Saoubi, Jon Andersson (Seco Tools AB, Sweden)
The effect of Si content on TiSiN and TiAlN/TiSiN films’ mechanical strength, brittleness, fatigue and adhesion is introduced. These films were deposited on cemented carbide inserts using cathodic arc evaporation method. Moreover, cutting performance investigations in milling stainless steel by these inserts are presented. According to previous research works, the addition of Si would lead to a linear PVD film structure, since the columnar one of a standard TiAlN coating is substituted by a dense nano-composite structure. Thus, on one hand, TiSiN films may possess improved mechanical properties in comparison to TiAlN ones. On the other hand, the adhesion of TiSiN films compared to TiAlN coatings is deteriorated. For overcoming potential film adhesive failures when cutting with TiSiN coated inserts, an adhesive TiAlN layer prior to the TiSiN film is deposited. In this way, it was possible to investigate the influence of the Si-content on the wear behaviour of TiAlN/TiSiN coated tools at the same adhesion quality level, as that of TiAlN films on cemented carbide inserts. In the conducted investigations, specimens coated with TiAlN/TiSiN films of various Si-contents were applied. For determining coating strength properties, nanoindentations were carried out. Based on these data and a FEM continuous simulation of nanoindentation, films’ elasto-plastic laws were determined. Moreover, nano-impact tests were conducted for capturing the influence of Si-content on TiSiN film brittleness. The fatigue properties of the examined coatings at ambient and elevated temperatures were encountered through perpendicular impact tests. The coatings’ adhesion was evaluated by inclined impact tests and by Rockwell indentations. Finally, milling experiments were carried out for investigating coated inserts cutting performance at various cutting speeds and consequently temperatures, using as workpiece material stainless steel 304 L. According to the obtained results, the beneficial effect of Si on the cutting performance of PVD coated tools was detected in an optimum cutting speed range. Moreover, a superficial TiSiN layer on TiAlN coated cemented carbide tools, leads to improved compound mechanical properties; these as well as the cutting performance depend on the TiSiN-film Si content.
11:20 AM G4-1+E-5 A Study on Friction and Wear Properties of Carbide Cutting Tools with MoS2 Coating Deposited by Electrostatic Spray Coating
UmaMaheshwera Reddy Paturi, Sureshkumarreddy Narala (BITS-Pilani, India)

In an attempt to explore the application of self-lubricant coatings on tribological components and to understand its influence in dry machining operations during tool-work sliding interaction, a laboratory based tribological simulation was conducted. To realize this, a wear test between Ti-6Al-4V alloy (counterface) and uncoated and coated cemented tungsten carbide-cobalt (WC-Co) alloy (pin specimen) at different sliding conditions was carried out using a pin-on-disc wear testing machine. The characteristics of wear rate, coefficient of friction and surface roughness were investigated with and without self-lubricant coatings on the carbide cutting tool specimen. In this work, electrostatic spray coating process was employed in deposition of molybdenum disulphide (MoS2) solid lubricant powder particles on specimens. Microstructure of specimen and counter surface was analyzed using scanning electron microscopy and optical microscopy. The results showed that the presence of solid lubricant film on specimen will greatly influence the sliding performance and improves the wear resistance through reduction in the mechanical energy given in the sliding contact due to presence of MoS2 lamellar structure as a transfer film.

Keywords: cemented carbide, solid lubricant, electrostatic spray coating, wear rate, friction, sliding performance

11:40 AM G4-1+E-6 Enhanced Cutting Performance of Tools Coated with Al2O3 –Based Coatings
Mojmir Jilek, Michel Sima (SHM, Czech Republic); Vladimir Maixner (Pramet Tools, Czech Republic)

From the point of view of oxidation and high-temperature wear resistance, Al2O3-based coatings are among the best available. This is especially useful for dry high-speed milling or turning of materials from the groups M 10 – 25 and K 10 – 20. We will report about the preparation and cutting performance of (Al1-xCrx)2O3 coatings deposited by vacuum arc technology in the coating system PLATIT π311, which uses rotating cylindrical cathodes made of pure Al and Cr targets in an oxygen-containing reactive gas atmosphere, where poisoning of the Al cathode was controlled by the deposition of metallic Cr onto the Al cathode surface . This procedure significantly improved the uniformity of the erosion of the Al cathode and reduced the roughness of the deposited coatings. The deposited coatings have been evaluated in terms of their surface roughness, hardness, and structure. The life time of tools coated wi th the new Al2O3-based coating during machining has been compared with other coatings.

Time Period MoM Sessions | Abstract Timeline | Topic G Sessions | Time Periods | Topics | ICMCTF2013 Schedule